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You know I'm in the preparation stage for a demo-mix too, so I know what you're talking about 
Basically, first find the records that you definetely want to include, just mess around as much as you can with them, try a lot of different transitions, see which tracks go well with each other. Then you can add other tracks later if you need to. Sometimes you have a lot of good tracks you want to play, but you need a filler track to for instance slow the mix down a bit. Lastly I suggest practicing some of the harder transtions, so that you know exactly when to bring in the new track.
Also, the mix I'm going to do will be my first 3-deck mix, which means that I'll try to have two tunes running at the same time most of the time. Not easy AT ALL, you have to concentrate all the time and there's no time for record hunting, have them lined up! The good thing is that if you experiment a lot you'll find tracks that when played together makes up a great, unique tune, and that can sound amazing (and impressive). Additionally I plan to use some acapellas during transitions ++. It's not going to be easy, but I'll do me best. There are so many "OK" DJs out there that you really have to do something special to be noticed.
Good luck!
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